{"id":218,"date":"2017-11-25T06:10:19","date_gmt":"2017-11-25T06:10:19","guid":{"rendered":"http:\/\/www-bfc.mls.eng.osaka-u.ac.jp\/ItohLab\/?page_id=218"},"modified":"2019-02-08T16:00:00","modified_gmt":"2019-02-08T07:00:00","slug":"equipments","status":"publish","type":"page","link":"http:\/\/www-bfc.mls.eng.osaka-u.ac.jp\/ItohLab\/?page_id=218","title":{"rendered":"Equipments\/\u8a2d\u5099"},"content":{"rendered":"
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    1. <\/a><\/li>\n\t\t\t\t\t\t\t\t\t\t\t
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    13. <\/a><\/li>\n\t\t\t\t\t\t\t\t\t<\/ol>\n\n\t\t\t\t
      \n\t\t\t\t\t\n\t\t\t\t\t\t<\/em>\n\t\t\t\t\t<\/a>\n\t\t\t\t<\/div>\n\n\t\t\t\t
      \n\t\t\t\t\t\n\t\t\t\t\t\t<\/em>\n\t\t\t\t\t<\/a>\n\t\t\t\t<\/div>\n\t\t\t\t<\/div><\/div><\/div><\/div><\/div>
      \n\n
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      \n
      \n\t

      Photo-dyode array system enables us to follow rapid reaction finishing within 50 sec.
      The cryostat guarantees stable reaction temperature from \u2013130 to 100\u00baC.
      This apparatus has developed by strong collaboration between Unisoku company and us, and spread to all over the world.
      Most part of our kinetic measurement was conducted with this equipment.
      Measurable wave length; 250\u20131000nm
      Minimum shutter speed; 0.5 s<\/p>\n

      \u53cd\u5fdc\u3092\u8ffd\u8de1\u3059\u308b\u969b\u306b\u3001\u8272\u306e\u5909\u5316\u3092\u89b3\u5bdf\u3059\u308b\u3053\u3068\u306f\u975e\u5e38\u306b\u5f37\u529b\u306a\u624b\u6bb5\u3067\u3059\u3002\u3053\u308c\u306f\u7d2b\u5916\u7dda\u304b\u3089\u8fd1\u8d64\u5916\u9818\u57df\u306e\u30b9\u30da\u30af\u30c8\u30eb\u5909\u5316\u3092\u8a18\u9332\u3059\u308b\u305f\u3081\u306e\u5206\u5149\u5668\u3067\u3059\u3002\u30d5\u30a9\u30c8\u30c0\u30a4\u30aa\u30fc\u30c9\u30a2\u30ec\u30a4\u5f0f\u306e\u30bb\u30f3\u30b5\u30fc\u3092\u642d\u8f09\u3057\u3066\u304a\u308a\u3001\u30cf\u30a4\u30b9\u30d4\u30fc\u30c9\u30ab\u30e1\u30e9\u306e\u3088\u3046\u306b\u4e00\u77ac\u3067\u5e83\u3044\u7bc4\u56f2\u306e\u30b9\u30da\u30af\u30c8\u30eb\u3092\u53d6\u5f97\u3059\u308b\u3053\u3068\u304c\u3067\u304d\u308b\u305f\u3081\u3001100\u79d2\u3067\u7d42\u308f\u3063\u3066\u3057\u307e\u3046\u3088\u3046\u306a\u53cd\u5fdc\u3082\u8ffd\u8de1\u3059\u308b\u3053\u3068\u304c\u53ef\u80fd\u3067\u3059\u3002
      \u307e\u305f\u3001\u30af\u30e9\u30a4\u30aa\u30b9\u30bf\u30c3\u30c8\u3092\u4f5c\u52d5\u3059\u308b\u3053\u3068\u3067\u3001-130~100\u2103\u306e\u6e29\u5ea6\u9818\u57df\u3067\u5b89\u5b9a\u306b\u30b9\u30da\u30af\u30c8\u30eb\u3092\u53d6\u5f97\u3059\u308b\u3053\u3068\u304c\u51fa\u6765\u307e\u3059\u3002
      \u3053\u306e\u7d44\u307f\u5408\u308f\u305b\u306f\u3001\u30e6\u30cb\u30bd\u30af\u793e\u3068\u6211\u3005\u306e\u5171\u540c\u958b\u767a\u3067\u751f\u307e\u308c\u3001\u4e16\u754c\u4e2d\u306e\u7814\u7a76\u5ba4\u306b\u5e83\u307e\u3063\u3066\u3086\u304d\u307e\u3057\u305f\u3002
      \u6211\u3005\u306f\u56db\u53f0\u3001\u3053\u306e\u88c5\u7f6e\u3092\u6240\u6709\u3057\u3066\u304a\u308a\u3001\u901f\u5ea6\u8ad6\u89e3\u6790\u306e\u30c7\u30fc\u30bf\u306e\u591a\u304f\u306f\u3053\u306e\u88c5\u7f6e\u3067\u6e2c\u5b9a\u3055\u308c\u3066\u3044\u307e\u3059\u3002
      \u6e2c\u5b9a\u6ce2\u9577\u9818\u57df; 250\u20131000 nm
      \u6e2c\u5b9a\u9593\u9694; 0.5 s<\/p>\n<\/div>\n<\/div><\/div><\/div><\/div>

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      Glove Box (Kiyon and Miwa*2)<\/h3>\n
      \n\t

      These boxes are filled with inert gas (nitrogen or argon).
      We can handle oxygen sensitive or moisture sensitive compounds in the boxes without special care and techniques. One of the boxes has a gas purification system tolerant\u00a0for \u00a0halogen solvents. We allow to use water in one of the boxes .<\/p>\n

      \u3053\u308c\u3089\u306e\u7bb1\u306e\u4e2d\u306f\u3001\u7a92\u7d20\u3084\u30a2\u30eb\u30b4\u30f3\u306a\u3069\u306e\u4e0d\u6d3b\u6027\u30ac\u30b9\u3067\u6e80\u305f\u3055\u308c\u3066\u3044\u308b\u306e\u3067\u3001
      \u3053\u306e\u88c5\u7f6e\u306e\u4e2d\u3067\u306f\u9178\u7d20\u3084\u6c34\u3067\u58ca\u308c\u3066\u3057\u307e\u3046\u3088\u3046\u306a\u5316\u5408\u7269\u3092\u3001\u5bb9\u6613\u306b\u6271\u3046\u3053\u3068\u304c\u51fa\u6765\u307e\u3059\u3002
      \u7bb1\u306e\u3046\u3061\u3001\u4e00\u3064\u306f\u30cf\u30ed\u30b2\u30f3\u7cfb\u6eb6\u5a92\u3092\u3064\u304b\u3046\u3053\u3068\u304c\u51fa\u6765\u307e\u3059\u3002\u307e\u305f\u3001\u4e00\u3064\u306f\u6c34\u3092\u4e2d\u3067\u7528\u3044\u3066\u3082\u826f\u3044\u3053\u3068\u306b\u3057\u3066\u3044\u307e\u3059\u3002<\/p>\n<\/div>\n<\/div><\/div><\/div><\/div>

      \n\n
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      CSI-TOF\/MS (Buruker)<\/h3>\n
      \n\t

      This spectrometer has electrospray on the injection unit and time-of-flight type detector which are suitable \u00a0for coordination compounds composed by \u00a0relatively week coordination bonds with large molecular weight. We also can analyze unstable compounds with special attachment, Cold Spray Ionizer (CSI), by decreasing the temperature of sprayer.
      Mass range 50 \u2013 20,000 m\/z
      Mass resolution 16,500 FWHM with micrOTOF focus
      Mass accuracy of < 1-2 ppm (RMS) error with internal calibration\u00a0<\/p>\n

      \u81ea\u5206\u306e\u5408\u6210\u3057\u305f\u672a\u77e5\u306e\u5206\u5b50\u304c\u3001\u3069\u3093\u306a\u3082\u306e\u3067\u3042\u308b\u304b\u660e\u3089\u304b\u306b\u3059\u308b\u306e\u306f\u3001\u3068\u3066\u3082\u5927\u5909\u306a\u9053\u306e\u308a\u3067\u3059\u3002\u73fe\u4ee3\u306e\u5316\u5b66\u7269\u8cea\u540c\u5b9a\u306f\u3001\u5404\u7a2e\u5206\u5149\u3068\u8cea\u91cf\u5206\u6790\u306e\u7d44\u307f\u5408\u308f\u305b\u306b\u3088\u308a\u3001\u5927\u304d\u304f\u524d\u9032\u3057\u307e\u3059\u3002
      \u3053\u306e\u88c5\u7f6e\u306e\u30a4\u30aa\u30f3\u5316\u90e8\u306f\u30a8\u30ec\u30af\u30c8\u30ed\u30b9\u30d7\u30ec\u30a4\u65b9\u5f0f\u3067\u3001\u3053\u308c\u306f\u6700\u3082\u30bd\u30d5\u30c8\u306a\u30a4\u30aa\u30f3\u5316\u6cd5\u3067\u3059\u3002\u8cea\u91cf\u5206\u6790\u90e8\u306f\u5206\u5b50\u304c\u98db\u884c\u3059\u308b\u6642\u9593\u304b\u3089m\/z\u3001\u3059\u306a\u308f\u3061\u5206\u5b50\u91cf\u3068\u96fb\u8377\u306e\u6bd4\u3092\u6c7a\u5b9a\u3059\u308bTime of flight \u578b\u3068\u306a\u3063\u3066\u3044\u307e\u3059\u3002TOF\u306f\u5e83\u3044\u7bc4\u56f2\u306e\u8cea\u91cf\u306b\u308f\u305f\u3063\u3066\u7cbe\u5bc6\u306a\u8cea\u91cf\u5206\u6790\u3092\u884c\u3046\u3053\u3068\u304c\u51fa\u6765\u308b\u691c\u51fa\u6cd5\u3067\u3059\u3002\u3059\u306a\u308f\u3061\u672c\u88c5\u7f6e\u306f\u3001\u6bd4\u8f03\u7684\u5f31\u3044\u7d50\u5408\u304b\u3089\u5f62\u6210\u3055\u308c\u3066\u304a\u308a\u3001\u5206\u5b50\u91cf\u306e\u5927\u304d\u306a\u9077\u79fb\u91d1\u5c5e\u932f\u4f53\u306e\u6e2c\u5b9a\u306b\u3001\u6700\u3082\u9069\u3057\u305f\u30bb\u30c3\u30c8\u30a2\u30c3\u30d7\u3068\u306a\u3063\u3066\u3044\u307e\u3059\u3002
      \u307e\u305f\u3001\u5c02\u7528\u306e\u30a2\u30bf\u30c3\u30c1\u30e1\u30f3\u30c8\u3092\u3064\u3051\u308b\u3053\u3068\u306b\u3088\u3063\u3066\u3001\u6e2c\u5b9a\u6e29\u5ea6\u3092\u4e0b\u3052\u308b\u3053\u3068\u304c\u3067\u304d\u3001\u5ba4\u6e29\u3067\u3059\u3050\u306b\u5206\u89e3\u3057\u3066\u3057\u307e\u3046\u3088\u3046\u306a\u4e0d\u5b89\u5b9a\u5316\u5408\u7269\u3084\u3001\u7d50\u5408\u5b9a\u6570\u306e\u975e\u5e38\u306b\u5c0f\u3055\u3044\u8d85\u5206\u5b50\u306e\u6e2c\u5b9a\u3092\u884c\u3046\u3053\u3068\u3082\u53ef\u80fd\u3067\u3059\u3002<\/p>\n<\/div>\n<\/div><\/div><\/div><\/div>

      \n\n
      \n\t\t\"\"\n\t<\/div>\n\n<\/div><\/div><\/div>

      GC-FID (Shimazu: GC-2010)<\/h3>\n
      \n\t

      This gas chromatograph is the main player in the evaluation of catalytic ability of the synthesized compounds. This machine is\u00a0equipped with auto-sampler. Quantification of the oxidation product is conducted with this machine almost all the day.<\/p>\n

      \u30b5\u30f3\u30d7\u30eb\u306e\u4e2d\u306e\u5316\u5408\u7269\u3092\u5206\u96e2\u3057\u3001\u305d\u308c\u305e\u308c\u3092\u540c\u5b9a\u3059\u308b\u306e\u306f\u5316\u5b66\u7814\u7a76\u306e\u8981\u3067\u3059\u3002\u3053\u306e\u88c5\u7f6e\u3067\u306f\u3001100\u2103\u4ee5\u4e0a\u306b\u71b1\u305b\u3089\u308c\u305f\u30ad\u30e3\u30d4\u30e9\u30ea\u30fc\u30ab\u30e9\u30e0\uff08\u5f84\u304c\u975e\u5e38\u306b\u7d30\u304f\u3066\u9577\u3044\uff09\u3067\u6709\u6a5f\u7269\u3092\u5206\u96e2\u3057\u3001FID\u3067\u691c\u51fa\u3057\u307e\u3059\u3002
      \u30aa\u30fc\u30c8\u30b5\u30f3\u30d7\u30e9\u30fc\u4ed8\u304d\u306a\u306e\u3067\u3001\u30b5\u30f3\u30d7\u30eb\u3092\u30bb\u30c3\u30c8\u3059\u308c\u3070\u305d\u306e\u5f8c\u306f\u5168\u81ea\u52d5\uff01\u9178\u5316\u53cd\u5fdc\u751f\u6210\u7269\u306e\u5b9a\u91cf\u3067\u3001\u5e73\u65e5\u306f\u307b\u307c\u305a\u3063\u3068\u7a3c\u50cd\u3057\u3066\u3044\u307e\u3059\u3002<\/p>\n<\/div>\n<\/div><\/div><\/div><\/div>

      \n\n
      \n\t\t\"\"\n\t<\/div>\n\n<\/div><\/div><\/div>

      Auto-flash column system (Yamazen Co.)<\/h3>\n
      \n\t

      This equipment can separate ca. 5 g of organic compound, automatically. Fractions are monitored by UV light and collected into sample tubes. Appropriate gradient of the solvents is expected by patent of Yamazen Co. with Rf values of TLC.<\/p>\n

      \u5408\u6210\u3057\u305f\u5316\u5408\u7269\u3092\u5206\u96e2\u3059\u308b\u306e\u306f\u3001\u306a\u304b\u306a\u304b\u5927\u5909\u306a\u4f5c\u696d\u3067\u3059\u3002\u30ab\u30e9\u30e0\u3092\u4f7f\u3063\u305f\u751f\u6210\u4f5c\u696d\u306f\u6642\u3068\u3057\u3066\u3001\u4e00\u6642\u9593\u4ee5\u4e0a\u3001\u5b9f\u9a13\u53f0\u306e\u524d\u306b\u5f35\u308a\u4ed8\u3044\u3066\u3044\u308b\u5fc5\u8981\u304c\u3042\u308a\u307e\u3059\u3002\u3053\u306e\u30d5\u30e9\u30c3\u30b7\u30e5\u30af\u30ed\u30de\u30c8\u306e\u30b7\u30b9\u30c6\u30e0\u306f\u3001\u30ab\u30e9\u30e0\u3092\u901a\u3063\u3066\u304d\u305f\u30b5\u30f3\u30d7\u30eb\u6eb6\u6db2\u3092UV\u3067\u5e38\u6642\u89b3\u5bdf\u3057\u3066\u304a\u308a\u3001UV\u306e\u5438\u53ce\u304c\u5909\u5316\u3057\u305f\u6240\u3067\u7570\u306a\u308b\u30b5\u30f3\u30d7\u30eb\u7ba1\u3078\u3068\u81ea\u52d5\u7684\u306b\u6eb6\u6db2\u3092\u53d6\u308a\u5206\u3051\u3066\u304f\u308c\u307e\u3059\u3002\u307e\u305f\u3001\u5c71\u5584\u306e\u7279\u8a31\u6280\u8853\u3067\u3001TLC\u306e\u30b9\u30dd\u30c3\u30c8\u304b\u3089\u5206\u96e2\u306b\u6700\u9069\u306a\u6eb6\u5a92\u306e\u30b0\u30e9\u30b8\u30a8\u30f3\u30c8\u3092\u4e88\u6e2c\u3059\u308b\u3053\u3068\u304c\u3067\u304d\u308b\u306e\u3067\u3001\u3088\u308a\u77ed\u3044\u6642\u9593\u3001\u5c11\u306a\u3044\u6eb6\u5a92\u91cf\u3067\u3001\u76ee\u7684\u306e\u5316\u5408\u7269\u3092\u5206\u96e2\u3059\u308b\u3053\u3068\u304c\u51fa\u6765\u307e\u3059\u3002\u4f0a\u6771\u7814\u3067\u306f\u3001\u307e\u305a\u53e4\u5178\u7684\u306a\u30ab\u30e9\u30e0\u306e\u624b\u6cd5\u3092\u4f53\u306b\u53e9\u304d\u8fbc\u307f\u3001\u539f\u7406\u3092\u7406\u89e3\u3057\u3066\u304b\u3089\u3053\u306e\u3088\u3046\u306a\u88c5\u7f6e\u3092\u4f7f\u3046\u3053\u3068\u306b\u3057\u3066\u3044\u307e\u3059\u3002<\/p>\n<\/div>\n<\/div><\/div><\/div><\/div>

      \n\n
      \n\t\t\"\"\n\t<\/div>\n\n<\/div><\/div><\/div>

      Rotary Evaporator (Vacuubrand)<\/h3>\n
      \n\t

      Once you set the pressure in the flask, the pressure inside flask is automatically stabilized with a\u00a0electromagnetic valve.<\/p>\n

      \u5316\u5408\u7269\u3092\u30ab\u30e9\u30e0\u306a\u3069\u3067\u751f\u6210\u3057\u305f\u3089\u3001\u30b5\u30f3\u30d7\u30eb\u3092\u6e2c\u5b9a\u306b\u56de\u3057\u305f\u308a\u3001\u4fdd\u5b58\u3059\u308b\u524d\u306b\u3001\u6eb6\u5a92\u3092\u53d6\u308a\u9664\u304f\u5de5\u7a0b\u304c\u5f85\u3063\u3066\u3044\u307e\u3059\u3002\u30d5\u30e9\u30b9\u30b3\u3092\u52a0\u71b1\u3059\u308b\u3068\u540c\u6642\u306b\u3001\u4e2d\u306e\u5727\u529b\u3092\u4e0b\u3052\u308b\u3053\u3068\u3067\u6eb6\u5a92\u306e\u901f\u3084\u304b\u306a\u84b8\u767a\u3092\u4fc3\u3057\u307e\u3059\u3002\u6c17\u5316\u3057\u305f\u6eb6\u5a92\u306f\u3001\u3082\u3046\u4e00\u5ea6\u51b7\u3084\u3055\u308c\u3066\u6db2\u5316\u3057\u3001\u4ed6\u306e\u30d5\u30e9\u30b9\u30b3\u3078\u3068\u96c6\u3081\u3089\u308c\u307e\u3059\u3002\u3053\u306e\u6642\u3001\u30d5\u30e9\u30b9\u30b3\u5185\u306e\u5727\u529b\u3092\u4e00\u5b9a\u306b\u4fdd\u3064\u3053\u3068\u304c\u3001\u52b9\u7387\u306e\u826f\u3044\u6eb6\u5a92\u7559\u53bb\u306b\u306f\u6b20\u304b\u305b\u307e\u305b\u3093\u304c\u3001\u30d5\u30e9\u30b9\u30b3\u3092\u305a\u3063\u3068\u898b\u5b88\u3063\u3066\u3044\u308b\u306e\u3082\u306a\u304b\u306a\u304b\u82e6\u75db\u306a\u5de5\u7a0b\u3067\u3059\u3002\u3053\u306e\u6a5f\u68b0\u306b\u306f\u3001\u5727\u529b\u8abf\u6574\u30e6\u30cb\u30c3\u30c8\u304c\u4ed8\u3044\u3066\u3044\u308b\u306e\u3067\u3001\u4e00\u5ea6\u30bb\u30c3\u30c8\u3057\u3066\u3057\u307e\u3048\u3070\u3001\u4ed6\u306e\u4f5c\u696d\u306b\u53d6\u308a\u639b\u304b\u308b\u3053\u3068\u304c\u51fa\u6765\u307e\u3059\u3002\u3068\u306f\u3044\u3048\u3001\u30d5\u30e9\u30b9\u30b3\u306e\u653e\u7f6e\u306f\u53b3\u7981\u3067\u3059\u3002<\/p>\n<\/div>\n<\/div><\/div><\/div><\/div>

      \n\n
      \n\t\t\"\"\n\t<\/div>\n\n<\/div><\/div><\/div>

      X-ray Diffractometer (Rigaku)<\/h3>\n
      \n\t

      Diffractometer for single crystal X-ray analysis. Powerful X-ray souse, VariMax. \u00a0on this machine enable us to analyze very small crystal (ca. 0.02 mm).<\/p>\n

      \u5358\u7d50\u6676X\u7dda\u69cb\u9020\u89e3\u6790\u306f\u3001\u5408\u6210\u3057\u305f\u5316\u5408\u7269\u306b\u3064\u3044\u3066\u8abf\u3079\u308b\u306b\u306f\u6700\u3082\u5f37\u529b\u306a\u6e2c\u5b9a\u624b\u6cd5\u306e\u4e00\u3064\u3067\u3059\u3002\u672c\u88c5\u7f6e\u306f\u5f37\u529b\u306aX\u7dda\u6e90\u3092\u642d\u8f09\u3057\u3066\u3044\u308b\u305f\u3081\u3001\u901a\u5e38\u306e\u88c5\u7f6e\u3067\u306f\u96e3\u3057\u3044\u3001\u5c0f\u3055\u306a\u7d50\u6676\u3067\u3082\u5341\u5206\u306b\u30af\u30aa\u30ea\u30c6\u30a3\u306e\u9ad8\u3044\u30c7\u30fc\u30bf\u3092\u5f97\u308b\u3053\u3068\u304c\u3067\u304d\u307e\u3059\u3002\u5408\u6210\u3057\u305f\u5316\u5408\u7269\u306e\u69cb\u9020\u304c\u5206\u304b\u308b\u77ac\u9593\u306f\u3001\u5316\u5b66\u8005\u3068\u3057\u3066\u7121\u4e0a\u306e\u559c\u3073\u3092\u611f\u3058\u308b\u3053\u3068\u306e\u3067\u304d\u308b\u4e00\u77ac\u3067\u3059\u3002<\/p>\n<\/div>\n<\/div><\/div><\/div><\/div>

      \n\n
      \n\t\t\"\"\n\t<\/div>\n\n<\/div><\/div><\/div>

      Stopped Flow Spectrometer (Unisoku)<\/h3>\n
      \n\t

      You can follow spectral changes finishing in 0.2 seconds with this machine. This apparatus has cooling unit enabling a measurement \u00a0under\u00a0\u2013100\u00baC conditions.<\/p>\n

      \u3053\u306e\u30b9\u30c8\u30c3\u30d7\u30c8\u30d5\u30ed\u30fc\u5206\u5149\u5149\u5ea6\u8a08\u306f\u3001\u6df7\u305c\u305f\u77ac\u9593\u306b\u7d42\u4e86\u3057\u3066\u3057\u307e\u3046\u3088\u3046\u306a\u9ad8\u901f\u306a\u53cd\u5fdc\u3092\u8ffd\u8de1\u3059\u308b\u305f\u3081\u306e\u88c5\u7f6e\u3067\u3059\u3002\u30ac\u30b9\u5727\u3067\u52d5\u4f5c\u3059\u308b\u30b7\u30ea\u30f3\u30c0\u30fc\u306b\u3088\u308a\u3001\u30b5\u30f3\u30d7\u30eb\u6eb6\u6db2\u304c\u7d20\u65e9\u304f&\u78ba\u5b9f\u306b\u6df7\u5408\u3055\u308c\u308b\u306e\u30670.2\u79d2\u7a0b\u5ea6\u3067\u7d42\u308f\u3063\u3066\u3057\u307e\u3046\u3088\u3046\u306a\u53cd\u5fdc\u3067\u3082\u3001\u8ffd\u8de1\u3059\u308b\u3053\u3068\u304c\u51fa\u6765\u307e\u3059\u3002\u6eb6\u6db2\u3092\u3055\u3089\u306b\u51b7\u5374\u3059\u308b\uff08\u2013100\u00baC\uff09\u3053\u3068\u3082\u53ef\u80fd\u3067\u3059\u3002<\/p>\n<\/div>\n<\/div><\/div><\/div><\/div>

      \n\n
      \n\t\t\"\"\n\t<\/div>\n\n<\/div><\/div><\/div>

      Absorption Spectrometer & Spectrofluorometer (JASCO)<\/h3>\n
      \n\t

      This absorption spectrometer can measure spectra up to 2500 nm with low temperature unit.<\/p>\n

      \u5149\u304c\u7269\u8cea\u306b\u5f53\u305f\u308b\u3068\u3001\u5149\u304c\u5438\u53ce\u3055\u308c\u305f\u308a\u3001\u5149\u3092\u653e\u3063\u305f\u308a\u3001\u7269\u8cea\u306e\u6027\u8cea\u3092\u53cd\u6620\u3057\u305f\u73fe\u8c61\u304c\u89b3\u5bdf\u3055\u308c\u307e\u3059\u3002\u3053\u308c\u3089\u306f\u3001\u3069\u306e\u3088\u3046\u306a\u6ce2\u9577\u306e\u5149\u3092\u3069\u308c\u304f\u3089\u3044\u5438\u3046\u304b\u5206\u6790\u3059\u308b\u5438\u5149\u5149\u5ea6\u8a08\u3068\u3001\u3069\u306e\u3088\u3046\u306a\u6ce2\u9577\u306e\u5149\u3092\u767a\u3059\u308b\u304b\u5206\u6790\u3059\u308b\u86cd\u5149\u5149\u5ea6\u8a08\u3067\u3059\u3002\u5438\u5149\u5149\u5ea6\u8a08\u306f2500nm\u306e\u8fd1\u8d64\u5916\u9818\u57df\u307e\u3067\u6e2c\u5b9a\u304c\u53ef\u80fd\u3067\u3059\u3002\u307e\u305f\u3001unisoku\u306e\u4f4e\u6e29\u6e2c\u5b9a\u30e6\u30cb\u30c3\u30c8\u3082\u8a2d\u7f6e\u53ef\u80fd\u3067\u3059\u3002<\/p>\n<\/div>\n<\/div><\/div><\/div><\/div>

      \n\n
      \n\t\t\"\"\n\t<\/div>\n\n<\/div><\/div><\/div>

      Deep Freezer<\/h3>\n
      \n\t

      Most of crystals unstable in room temperature is grown in this freezer.\u00a0Temperature: \u201360 \u00baC<\/p>\n

      \u4f0a\u6771\u7814\u3067\u306f\u5ba4\u6e29\u3067\u306f\u5206\u89e3\u3057\u3066\u3057\u307e\u3046\u3088\u3046\u306a\u3001\u6d3b\u6027\u4e2d\u9593\u4f53\u3092\u6349\u3048\u308b\u3053\u3068\u306b\u3082\u30c1\u30e3\u30ec\u30f3\u30b8\u3057\u3066\u3044\u307e\u3059\u3002\u591a\u304f\u306e\u5834\u5408\u3001\u7d50\u6676\u306f\u3053\u306e\u2013\uff16\uff10\u2103\u306e\u51b7\u8535\u5eab\u306e\u4e2d\u3067\u80b2\u3066\u3089\u308c\u3066\u3044\u307e\u3059\u3002<\/p>\n<\/div>\n<\/div><\/div><\/div><\/div>

      \n\n
      \n\t\t\"\"\n\t<\/div>\n\n<\/div><\/div><\/div>

      Workstation (HPC systems)<\/h3>\n
      \n\t

      Intel(R) Xeon(R) CPU E5-2687W 0 @ 3.10GHz
      16 cores
      MemTotal: \u00a0 \u00a0 \u00a0 65939904 kB<\/p>\n

      \u6211\u3005\u306e\u7814\u7a76\u5ba4\u3067\u306f\u3001\u6271\u3063\u3066\u3044\u308b\u5316\u5408\u7269\u306e\u69cb\u9020\u3084\u4f38\u7e2e\u632f\u52d5\u3001\u8ecc\u9053\u3001\u5b89\u5b9a\u6027\u306b\u3064\u3044\u3066\u306e\u60c5\u5831\u3092\u5f97\u308b\u305f\u3081\u306b\u3001DFT\u8a08\u7b97\u3082\u884c\u3044\u307e\u3059\u300250\u539f\u5b50\u304f\u3089\u3044\u306e\u914d\u4f4d\u5316\u5408\u7269\u3067\u3042\u308c\u3070\u30016-311g(d)\u30ec\u30d9\u30eb\u3067\u306e\u3073\u306e\u3073\u8a08\u7b97\u3059\u308b\u3053\u3068\u304c\u51fa\u6765\u307e\u3059\u3002100\u304f\u3089\u3044\u306e\u5206\u5b50\u304b\u3089\u306f\u30fb\u30fb\u30fb\u8981\u76f8\u8ac7\u3067\u3059\u3002<\/p>\n<\/div>\n<\/div><\/div><\/div><\/div>

      \n\n
      \n\t\t\"\"\n\t<\/div>\n\n<\/div><\/div><\/div>

      Infrared Spectrometer (Simadzu)<\/h3>\n
      \n\t

      We can obtain IR spectra under low temperature conditions.<\/p>\n

      \u65b0\u3057\u3044\u307b\u3046\u306e\u8d64\u5916\u7dda\u5206\u5149\u5668\u3067\u3059\u3002\u4f4e\u6e29\u6e2c\u5b9a\u3082\u53ef\u80fd\u3002<\/p><\/div>\n<\/div><\/div><\/div><\/div>

      \n\n
      \n\t\t\"\"\n\t<\/div>\n\n<\/div><\/div><\/div>

      High Pressure Reactor<\/h3>\n
      \n\t

      This large apparatus is \u00a0for reactions under high pressure conditions up to 5.0 MPa. Currently, methane, ethane, propane, nitrogen, and oxygen gas flows are available. Notably, this system has a auto-sampler.<\/p>\n

      \u9ad8\u5727\u6761\u4ef6\u4e0b\u3067\u306e\u53cd\u5fdc\u3092\u884c\u3046\u5b9f\u9a13\u88c5\u7f6e\u3067\u3059\u300250\u6c17\u5727\u307e\u3067\u3001\u5727\u529b\u3092\u304b\u3051\u308b\u3053\u3068\u304c\u3067\u304d\u307e\u3059\u3002\u73fe\u5728\u3001\u30e1\u30bf\u30f3\u3001\u30a8\u30bf\u30f3\u3001\u30d7\u30ed\u30d1\u30f3\u30ac\u30b9\u3068\u7a92\u7d20\u3001\u9178\u7d20\u30ac\u30b9\u3092\u4f7f\u3046\u3053\u3068\u304c\u3067\u304d\u307e\u3059\u3002\u30aa\u30fc\u30c8\u30b5\u30f3\u30d7\u30e9\u30fc\u304c\u4ed8\u3044\u3066\u3044\u308b\u306e\u3067\u3001\u7d4c\u6642\u5909\u5316\u3082\u697d\u3005\u8ffd\u8de1\u53ef\u80fd\u3067\u3059\u3002<\/p>\n<\/div>\n<\/div><\/div><\/div><\/div>

      \t\t\t

      This page is under construction. We will soon add information of another equipments.<\/p>\n

      \u3053\u308c\u3089\u306f\u307e\u3060\u307e\u3060\u6a5f\u5668\u306e\u4e00\u90e8\u3067\u3059\u3002\u9806\u6b21\u3001\u8ffd\u52a0\u4e88\u5b9a\u3067\u3059\u3002<\/p>\n<\/div>\n\t\t<\/div><\/div><\/div><\/div>","protected":false},"excerpt":{"rendered":"

      Photo-dyode array system enables us to follow rapid reaction finishing within 50 sec. The cryostat guarantees stable reaction temperature from \u2013130 to 100\u00baC. This apparatus has developed by strong collaboration between Unisoku company and us, and spread to all over the world. Most part of our kinetic measurement was conducted with this equipment. Measurable wave … <\/p>\n

      Continue reading “Equipments\/\u8a2d\u5099”<\/span><\/a><\/p>\n","protected":false},"author":1,"featured_media":0,"parent":0,"menu_order":0,"comment_status":"closed","ping_status":"closed","template":"","meta":{"footnotes":""},"_links":{"self":[{"href":"http:\/\/www-bfc.mls.eng.osaka-u.ac.jp\/ItohLab\/index.php?rest_route=\/wp\/v2\/pages\/218"}],"collection":[{"href":"http:\/\/www-bfc.mls.eng.osaka-u.ac.jp\/ItohLab\/index.php?rest_route=\/wp\/v2\/pages"}],"about":[{"href":"http:\/\/www-bfc.mls.eng.osaka-u.ac.jp\/ItohLab\/index.php?rest_route=\/wp\/v2\/types\/page"}],"author":[{"embeddable":true,"href":"http:\/\/www-bfc.mls.eng.osaka-u.ac.jp\/ItohLab\/index.php?rest_route=\/wp\/v2\/users\/1"}],"replies":[{"embeddable":true,"href":"http:\/\/www-bfc.mls.eng.osaka-u.ac.jp\/ItohLab\/index.php?rest_route=%2Fwp%2Fv2%2Fcomments&post=218"}],"version-history":[{"count":60,"href":"http:\/\/www-bfc.mls.eng.osaka-u.ac.jp\/ItohLab\/index.php?rest_route=\/wp\/v2\/pages\/218\/revisions"}],"predecessor-version":[{"id":1778,"href":"http:\/\/www-bfc.mls.eng.osaka-u.ac.jp\/ItohLab\/index.php?rest_route=\/wp\/v2\/pages\/218\/revisions\/1778"}],"wp:attachment":[{"href":"http:\/\/www-bfc.mls.eng.osaka-u.ac.jp\/ItohLab\/index.php?rest_route=%2Fwp%2Fv2%2Fmedia&parent=218"}],"curies":[{"name":"wp","href":"https:\/\/api.w.org\/{rel}","templated":true}]}}